MS Report from Instrument: HY-LCMS-02 File D:\\CHEM32\\1\\DATA\\HEC\\HYQ4070-056-1.D Tgt Mass (EZX): Injection Date : 4 May 17 3:39 pm +0800 Seq. Line : 0 Sample Name : HYQ4070-056-1 Location : P1-E-05 Acq. Operator : CLJ_701 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No : HY-78961 Batch#25485 Easy-Access Method: '1-POS-3MIN' Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C*DAD1 B, Sig=214,4 Ref=off mAU2000150010001.5151.5472.63950000.5*DAD1 C, Sig=254,4 Ref=off mAU2520151050-50.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701000008000060000400002000000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5min1.51.73711.6081.51.60822.5min*1.6582.10922.5min* RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.51 0.02 4.05 3.19 0.15 ND 1.55 0.02 4.98 4.17 0.19 ND 1.61 0.02 2630.08 2268.85 99.37 309 2.64 0.05 7.57 2.47 0.29 159 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.61 0.02 35.14 32.70 96.45 ND 1.66 0.02 0.41 0.40 1.14 340 2.11 0.02 0.88 0.85 2.41 NDHY-LCMS-02 5/4/2017 5:14:13 PM CLJ_701Page 1 of 2
MS Report from Instrument: HY-LCMS-02
Ret. Time: 1.74 <<<< POSITIVE SPECTRA >>>> ES-API Positive160001400012000 331.0 194.1 310.1 332.01000080006000400020000200300400500600700800900m/z 309.1HY-LCMS-02 5/4/2017 5:14:13 PM CLJ_701Page 2 of 2
